Filename: C:\Program Files\PerkinElmer\Pyris\data\Indium 10252016.ds8d Operator ID: Jerry Sample ID: indium Comment: training Serial Number: 534L1608121 Data Collected: 10/25/2016 5:05:28 PM Sample Weight: 5.749 mg Display Weight: 5.749 Validation Validated: No By: Date: Calibration Information Filename: C:\Program Files\PerkinElmer\Pyris\Calibrations\October 25 2016 10C.ds8c Date/Time: 10/25/2016 3:52:47 PM Initial Conditions Temperature: 130.00 °C Purge Gas: Purge Gas Rate: Baseline Filename: End Condition: Go To Load Total Points in Run: 675 Method Steps: Pre-Run Actions Switch the Gas to Nitrogen at 20.0 ml/min Action occurs Immediately Start the Run Action occurs Immediately 1) Heat from 130.00°C to 175.00°C at 20.00°C/min 1) DSC 8500 Temperature Scan Time Unsubtracted Baseline Program Sample Approx. Heat Flow Uncorrected Heat Flow Heat Flow Temperature Temperature Gas Flow Calibration Heat Flow 0.000000 9.616795 0.000000 130.054000 130.662000 0.000000 1.075123 9.616795 0.003333 9.724953 0.000000 130.120000 130.662000 0.000000 1.075123 9.724953 0.006667 9.893962 0.000000 130.187000 130.662000 0.000000 1.075123 9.893962 0.010000 10.072647 0.000000 130.254000 130.670000 0.000000 1.075123 10.072647 0.013333 10.229830 0.000000 130.320000 130.683000 0.000000 1.075123 10.229830 0.016667 10.353577 0.000000 130.387000 130.708000 0.000000 1.075123 10.353577 0.020000 10.442705 0.000000 130.454000 130.737000 0.000000 1.075123 10.442705 0.023333 10.502159 0.000000 130.520000 130.775000 0.000000 1.075123 10.502159 0.026667 10.539573 0.000000 130.587000 130.816000 0.000000 1.075123 10.539573 0.030000 10.562473 0.000000 130.654000 130.862000 0.000000 1.075123 10.562473 0.033333 10.577847 0.000000 130.720000 130.916000 0.000000 1.075123 10.577847 0.036667 10.591824 0.000000 130.787000 130.970000 0.000000 1.075123 10.591824 0.040000 10.608703 0.000000 130.854000 131.033000 0.000000 1.075123 10.608703 0.043333 10.630958 0.000000 130.920000 131.100000 0.000000 1.075123 10.630958 0.046667 10.660739 0.000000 130.987000 131.162000 0.000000 1.075123 10.660739 0.050000 10.698799 0.000000 131.054000 131.225000 0.000000 1.075123 10.698799 0.053333 10.744599 0.000000 131.120000 131.291000 0.000000 1.075123 10.744599 0.056667 10.798570 0.000000 131.187000 131.358000 0.000000 1.075123 10.798570 0.060000 10.860282 0.000000 131.254000 131.420000 0.000000 1.075123 10.860282 0.063333 10.929090 0.000000 131.320000 131.487000 0.000000 1.075123 10.929090 0.066667 11.003381 0.000000 131.387000 131.554000 0.000000 1.075123 11.003381 0.070000 11.081435 0.000000 131.454000 131.620000 0.000000 1.075123 11.081435 0.073333 11.162822 0.000000 131.520000 131.687000 0.000000 1.075123 11.162822 0.076667 11.246144 0.000000 131.587000 131.754000 0.000000 1.075123 11.246144 0.080000 11.329251 0.000000 131.654000 131.820000 0.000000 1.075123 11.329251 0.083333 11.411605 0.000000 131.720000 131.883000 0.000000 1.075123 11.411605 0.086667 11.492132 0.000000 131.787000 131.954000 0.000000 1.075123 11.492132 0.090000 11.570293 0.000000 131.854000 132.016000 0.000000 1.075123 11.570293 0.093333 11.646197 0.000000 131.920000 132.083000 0.000000 1.075123 11.646197 0.096667 11.719628 0.000000 131.987000 132.150000 0.000000 1.075123 11.719628 0.100000 11.790048 0.000000 132.054000 132.216000 0.000000 1.075123 11.790048 0.103333 11.856813 0.000000 132.120000 132.283000 0.000000 1.075123 11.856813 0.106667 11.920568 0.000000 132.187000 132.345000 0.000000 1.075123 11.920568 0.110000 11.980775 0.000000 132.254000 132.412000 0.000000 1.075123 11.980775 0.113333 12.036574 0.000000 132.320000 132.479000 0.000000 1.075123 12.036574 0.116667 12.088717 0.000000 132.387000 132.545000 0.000000 1.075123 12.088717 0.120000 12.138388 0.000000 132.450000 132.612000 0.000000 1.075123 12.138388 0.123333 12.184618 0.000000 132.516000 132.679000 0.000000 1.075123 12.184618 0.126667 12.227838 0.000000 132.583000 132.745000 0.000000 1.075123 12.227838 0.130000 12.267833 0.000000 132.650000 132.812000 0.000000 1.075123 12.267833 0.133333 12.305462 0.000000 132.716000 132.875000 0.000000 1.075123 12.305462 0.136667 12.340188 0.000000 132.783000 132.941000 0.000000 1.075123 12.340188 0.140000 12.372872 0.000000 132.850000 133.008000 0.000000 1.075123 12.372872 0.143333 12.403190 0.000000 132.916000 133.075000 0.000000 1.075123 12.403190 0.146667 12.431251 0.000000 132.983000 133.141000 0.000000 1.075123 12.431251 0.150000 12.457699 0.000000 133.050000 133.208000 0.000000 1.075123 12.457699 0.153333 12.482965 0.000000 133.116000 133.275000 0.000000 1.075123 12.482965 0.156667 12.506510 0.000000 133.183000 133.341000 0.000000 1.075123 12.506510 0.160000 12.528120 0.000000 133.250000 133.404000 0.000000 1.075123 12.528120 0.163333 12.548440 0.000000 133.316000 133.470000 0.000000 1.075123 12.548440 0.166667 12.567469 0.000000 133.383000 133.537000 0.000000 1.075123 12.567469 0.170000 12.585531 0.000000 133.450000 133.604000 0.000000 1.075123 12.585531 0.173333 12.602626 0.000000 133.516000 133.670000 0.000000 1.075123 12.602626 0.176667 12.619398 0.000000 133.583000 133.733000 0.000000 1.075123 12.619398 0.180000 12.635524 0.000000 133.650000 133.800000 0.000000 1.075123 12.635524 0.183333 12.651436 0.000000 133.716000 133.870000 0.000000 1.075123 12.651436 0.186667 12.666703 0.000000 133.783000 133.933000 0.000000 1.075123 12.666703 0.190000 12.681110 0.000000 133.850000 133.995000 0.000000 1.075123 12.681110 0.193333 12.694764 0.000000 133.916000 134.066000 0.000000 1.075123 12.694764 0.196667 12.707988 0.000000 133.983000 134.137000 0.000000 1.075123 12.707988 0.200000 12.720889 0.000000 134.050000 134.200000 0.000000 1.075123 12.720889 0.203333 12.733253 0.000000 134.116000 134.266000 0.000000 1.075123 12.733253 0.206667 12.744972 0.000000 134.183000 134.333000 0.000000 1.075123 12.744972 0.210000 12.755508 0.000000 134.250000 134.400000 0.000000 1.075123 12.755508 0.213333 12.765614 0.000000 134.316000 134.466000 0.000000 1.075123 12.765614 0.216667 12.774860 0.000000 134.383000 134.533000 0.000000 1.075123 12.774860 0.220000 12.783354 0.000000 134.450000 134.595000 0.000000 1.075123 12.783354 0.223333 12.791095 0.000000 134.516000 134.662000 0.000000 1.075123 12.791095 0.226667 12.798513 0.000000 134.583000 134.729000 0.000000 1.075123 12.798513 0.230000 12.805394 0.000000 134.650000 134.795000 0.000000 1.075123 12.805394 0.233333 12.811952 0.000000 134.716000 134.862000 0.000000 1.075123 12.811952 0.236667 12.818295 0.000000 134.783000 134.929000 0.000000 1.075123 12.818295 0.240000 12.824638 0.000000 134.850000 134.995000 0.000000 1.075123 12.824638 0.243333 12.830229 0.000000 134.916000 135.062000 0.000000 1.075123 12.830229 0.246667 12.834315 0.000000 134.979000 135.125000 0.000000 1.075123 12.834315 0.250000 12.838508 0.000000 135.045000 135.191000 0.000000 1.075123 12.838508 0.253333 12.843238 0.000000 135.112000 135.258000 0.000000 1.075123 12.843238 0.256667 12.847754 0.000000 135.179000 135.325000 0.000000 1.075123 12.847754 0.260000 12.852914 0.000000 135.245000 135.395000 0.000000 1.075123 12.852914 0.263333 12.858075 0.000000 135.312000 135.458000 0.000000 1.075123 12.858075 0.266667 12.862805 0.000000 135.379000 135.525000 0.000000 1.075123 12.862805 0.270000 12.867321 0.000000 135.445000 135.595000 0.000000 1.075123 12.867321 0.273333 12.871944 0.000000 135.512000 135.658000 0.000000 1.075123 12.871944 0.276667 12.876352 0.000000 135.579000 135.729000 0.000000 1.075123 12.876352 0.280000 12.881405 0.000000 135.645000 135.791000 0.000000 1.075123 12.881405 0.283333 12.886566 0.000000 135.712000 135.858000 0.000000 1.075123 12.886566 0.286667 12.891404 0.000000 135.779000 135.925000 0.000000 1.075123 12.891404 0.290000 12.896134 0.000000 135.845000 135.991000 0.000000 1.075123 12.896134 0.293333 12.901725 0.000000 135.912000 136.058000 0.000000 1.075123 12.901725 0.296667 12.907638 0.000000 135.979000 136.120000 0.000000 1.075123 12.907638 0.300000 12.913444 0.000000 136.045000 136.187000 0.000000 1.075123 12.913444 0.303333 12.918604 0.000000 136.112000 136.258000 0.000000 1.075123 12.918604 0.306667 12.924195 0.000000 136.179000 136.320000 0.000000 1.075123 12.924195 0.310000 12.930108 0.000000 136.245000 136.387000 0.000000 1.075123 12.930108 0.313333 12.936451 0.000000 136.312000 136.454000 0.000000 1.075123 12.936451 0.316667 12.942902 0.000000 136.379000 136.520000 0.000000 1.075123 12.942902 0.320000 12.949353 0.000000 136.445000 136.587000 0.000000 1.075123 12.949353 0.323333 12.955373 0.000000 136.512000 136.654000 0.000000 1.075123 12.955373 0.326667 12.961394 0.000000 136.579000 136.720000 0.000000 1.075123 12.961394 0.330000 12.967630 0.000000 136.645000 136.787000 0.000000 1.075123 12.967630 0.333333 12.974403 0.000000 136.712000 136.850000 0.000000 1.075123 12.974403 0.336667 12.980746 0.000000 136.779000 136.916000 0.000000 1.075123 12.980746 0.340000 12.987305 0.000000 136.845000 136.983000 0.000000 1.075123 12.987305 0.343333 12.993863 0.000000 136.912000 137.050000 0.000000 1.075123 12.993863 0.346667 13.000206 0.000000 136.979000 137.120000 0.000000 1.075123 13.000206 0.350000 13.006872 0.000000 137.045000 137.187000 0.000000 1.075123 13.006872 0.353333 13.013322 0.000000 137.112000 137.254000 0.000000 1.075123 13.013322 0.356667 13.020096 0.000000 137.179000 137.320000 0.000000 1.075123 13.020096 0.360000 13.026546 0.000000 137.245000 137.387000 0.000000 1.075123 13.026546 0.363333 13.032567 0.000000 137.312000 137.454000 0.000000 1.075123 13.032567 0.366667 13.038695 0.000000 137.379000 137.520000 0.000000 1.075123 13.038695 0.370000 13.044716 0.000000 137.441000 137.587000 0.000000 1.075123 13.044716 0.373333 13.051382 0.000000 137.508000 137.654000 0.000000 1.075123 13.051382 0.376667 13.058370 0.000000 137.575000 137.720000 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138.441000 138.579000 0.000000 1.075123 13.148573 0.423333 13.154379 0.000000 138.508000 138.650000 0.000000 1.075123 13.154379 0.426667 13.160722 0.000000 138.575000 138.716000 0.000000 1.075123 13.160722 0.430000 13.166742 0.000000 138.641000 138.783000 0.000000 1.075123 13.166742 0.433333 13.172763 0.000000 138.708000 138.850000 0.000000 1.075123 13.172763 0.436667 13.179321 0.000000 138.775000 138.920000 0.000000 1.075123 13.179321 0.440000 13.185665 0.000000 138.841000 138.983000 0.000000 1.075123 13.185665 0.443333 13.192975 0.000000 138.908000 139.050000 0.000000 1.075123 13.192975 0.446667 13.199964 0.000000 138.975000 139.116000 0.000000 1.075123 13.199964 0.450000 13.207490 0.000000 139.041000 139.179000 0.000000 1.075123 13.207490 0.453333 13.216091 0.000000 139.108000 139.250000 0.000000 1.075123 13.216091 0.456667 13.224047 0.000000 139.175000 139.316000 0.000000 1.075123 13.224047 0.460000 13.232002 0.000000 139.241000 139.379000 0.000000 1.075123 13.232002 0.463333 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0.000000 1.075123 17.424443 DSC8000 MANUAL TUNE CALIBRATION VALUES: Date: 10/25/2016 4:00:41 PM Slope: 50 Coarse Balance: 3 Fine Balance: 20 DSC8000 SMARTSCAN CALIBRATION VALUES: Date: 10/25/2016 9:58:14 AM SmartScan Enabled = No Calibration File: Starting Temperature: -50.0 °C Ending Temperature: 450.0 °C Number of Steps: 15 DSC8000 SAMPLE TEMPERATURE CALIBRATION VALUES: Date: 10/25/2016 3:21:48 PM Reference Expected (°C) Measured (°C) Weight (mg) Scan rate (°C/min) Method Indium 156.600 156.700 5.749 10.0 Zinc 419.470 418.850 3.041 10.0 NEWPAGE DSC8000 FURNACE TEMPERATURE CALIBRATION VALUES: Minimum -25.000 °C Maximum 600.000 °C FURNACE CALIBRATION COMPUTED RESULTS: Date: 10/25/2016 3:47:01 PM Setpoints (°C) Boundaries (°C) y'' -25.000 -23.609 0 53.125 54.516 -0.00010897 131.250 133.141 -5.0797e-005 209.375 212.162 -6.6983e-005 287.500 291.587 -6.2107e-005 365.625 371.412 -5.603e-005 443.750 451.604 -4.9697e-005 521.875 532.158 -7.1977e-005 600.000 613.091 0 DSC8000 HEAT FLOW CALIBRATION VALUES: Reference Temperature(°C) Expected(J/g) Measured(J/g) Weight(mg) Scan rate(°C/min) Indium 156.600 28.450 26.462 5.749 10.0 DSC8000 HEAT FLOW CALIBRATION COMPUTED RESULTS: Date: 10/25/2016 3:52:21 PM K(Ts) = (0)Ts^3 + (0)Ts^2 + (0)Ts + (1.0751) PROFILE VALUES FOR THIS DATA: Software Version 13.2.1.0007 Firmware Version Part Number N5368010 Revision 0.01:. Build 4 Instrument Serial Number 534L1608121 Load Temperature 30.0 °C Go To Temp Rate 200.0 °C/min Maximum Allowed Temperature 600.0 °C Helium Purge Was Not Used Liquid Nitrogen Was Not Used Data taken using the Normal Range Filter Factor 0 Cooling Device Intracooler II Wavelet Denoising used: No Autoslope Used: No