Filename: C:\Program Files\PerkinElmer\Pyris\data\ZINCCAL.DSD Operator ID: Applications Laboratory Sample ID: Zinc Comment: Ice Serial Number: Data Collected: 1/4/1996 3:40:08 PM Sample Weight: 2.002 mg Display Weight: 2.002 Validation Validated: No By: Date: Calibration Information Filename: N:\PD\PRODUCTS\PYRIS\DATA\BENS\DEFAULTS.DSC Date/Time: Initial Conditions Temperature: 370.00 °C Y Initial: 20.00 mW Sample Rate: Standard Baseline Filename: End Condition: Go To: 370.00°C Total Points in Run: 1760 Method Steps: Pre-Run Actions Switch the Gas to Nitrogen at 20.0 ml/min Action occurs Immediately Start the Run Action occurs Immediately 1) Heat from 370.00°C to 440.00°C at 10.00°C/min 1) DSC Temperature Scan Time Unsubtracted Baseline Program Sample Heat Flow Heat Flow Temperature Temperature 0.000000 20.000593 0.000000 370.000000 370.000000 0.003333 20.001482 0.000000 370.033000 370.033000 0.006667 20.002075 0.000000 370.066000 370.066000 0.010000 20.002667 0.000000 370.100000 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